STATISTICAL ANALYSIS OF THE RESULTS OF LABORATORY RESEARCH AS ONE OF THE METHODS OF INCREASING THE COMPETITIVENESS OF A MILK PROCESSING ENTERPRISE

Keywords: statistical analysis, intervals, hypothesis testing, mean square deviation, variance, competitiveness, milk processing enterprise

Abstract

Ensuring the stable quality of food products is the primary production for any enterprise, as well as a priority for government bodies whose activities aim to protect consumers and detect adulteration of consumer products. From time to time, food manufacturers receive complaints from buyers regarding the inconsistency of the content of individual indicators with those declared in the specification or on the label. The causality of such appeals can be intentional falsification of the product and non-compliance with the accuracy of research methods, usually due to low technical support of analytical laboratories of enterprises. That is why the statistical analysis of research results will allow the evaluation of the obtained product and establish its "compliance" with the buyers requirements. The articles purpose is a theoretical overview of individual statistical analysis methods of research and their practical application in the laboratory of a milk processing enterprise. The article examines using intervals as an element of statistical analysis of laboratory research results. The indicators of the average value and variance allow us to characterize both the studied sample and the methodology. An example of this is the analysis of the study results of the mass fraction of fat in milk by various analysis methods. The approach for testing hypotheses is also considered because, for any laboratory, it is necessary to understand whether the method of analysis applied to the selected sample provides a certified value. This issue is especially acute in the production laboratory during the incoming control of raw materials ingredients and during the study of the finished product. If, based on the experimental results, it is decided that the technique used is flawed, we conclude that it has a systematic error. Such errors will cause unreliable results, which will cause financial and reputational losses for the company. Given the complex situation in the dairy market of our country, such losses can be fatal for a milk processing enterprise, which is why it is necessary to provide a statistical analysis of the applied methods for confidence in our own products.

References

Білецький Е.В., Янушкевич Д.А., Шайхлісламов З.Р. Управління якістю продукції та послуг: навчальний посібник. Харків : ХТЕІ, 2015. 222с.

Савуляк В.В. Управління якістю продукції : навчальний посібник. Вінниця : ВНТУ, 2012. 91с.

Alewijn M., Vander Voet H., Van Ruth S. Validation of multivariate classification methods using analytical fingerprints-Concept and case study on organic feed for laying hens. Journal of Food Composition and Analysis. 2016. Vol. 51. Pр. 15–23.

Armstrong N., Hibbert D.B. An Introduction to Bayesian Methods for Analyzing Chemistry Data. Chemom. Intel. Lab. Syst. 2009. Part 1. Vol. 97. Pр. 194–210.

Medina S. Current trends and recent advances on food authenticity technologies and chemometric approaches. Trends in Food Science & Technology. 2019. Vol. 85. Pр. 163-176.

CX/FICS 18/24/7 Discussion paper on food integrity and food authenticity. Codex committee on food import and export inspection and certification systems. Twenty-Fourth Session. Brisbane, Australia, October 22-26, 2018.

Delgado-Aguilar M., Valverde-Som L., Cuadros-Rodríguez L. Solver, an Excel Application to Solve the Difficulty in Applying Different Univariate Linear Regression Methods. Chemom. Intell. Lab. Syst. 2018. Vol. 178. Pр. 39–46.

Herrero A. Determination of the Capability of Detection of a Hyphenated Method: Application to Spectroelectrochemistry. Chemom. Intell. Lab. Syst. 2002. Vol. 61. Pр. 63–74.

Dong W., Zhang Y., Zhang B. Quantitative analysis of adulteration of extra virgin olive oil using Raman spectroscopy improved by bayesin framework least squares support vector machines. Analytical Methods. 2012. Vol. 4. Pр. 2772–2777.

Feinberg M. Validation of Analytical Methods Based on Accuracy Profiles. Journal of Chromatography A. 2007. Vol. 1158. Pр. 174–183.

García I., Sarabia L., Ortiz M.C., Aldama J.M. Usefulness of D-optimal Designs and Multicriteria Optimization in Laborious Analytical Procedures. Application to the Extraction of Quinolones From Eggs. Journal of Chromatography A. 2005. Vol. 1085. Pр. 190–198.

González A.G., Herrador M.A. Accuracy Profiles from Uncertainty Measurements. Talanta. 2006. Vol. 70. Pр. 896–901.

Knowledge Centre for Food Fraud and Quality. URL: https://knowledge4policy.ec.europa.eu/food-fraud-quality/topic/food-fraud_en.

Huch C.W., Pezzei C.K., Huck-Pezzei V.A.C. An industry pespective of food fraud. Current Opinion in Food Science. 2016. Vol. 10. Pр. 32–37.

Kumar N., Bansal A., Sarma G.S. Chemometrics tools in analytical chemistry: An overview. Talanta. 2014. Vol. 123. Pр. 186–199.

Maning L. Food Fraud: policy and food chain. Current Opinion in Food Science. 2016. Vol. 10. Pр. 16–21.

Ortiz M.C., Herrero A., Sanllorente S., Reguera C. The Quality of the Information Contained in Chemical Measures. Servicio de Publicaciones Universidad de Burgos: Burgos. 2005.

Ortiz M.C., Sarabia L.A., Sánchez M.S. Tutorial on Evaluation of Type I and type II Errors in Chemical Analyses: From the Analytical Detection to Authentication of Products and Process Control. Anal. Chim. Acta. 2010. Vol. 674. Pр. 123–142.

Ortiz M.C., Sarabia L.A., Sánchez M.S., Herrero A. Quality of Analytical Measurements: Statistical Methods for Internal Validation. Chemical and Biochemical Data Analysis. 2020. Pр. 1–52.

Oca M. Robustness Testing in the Determination of Seven Drugs in Animal Muscle by Liquid Chromatography–Tandem Mass Spectrometry. Chemom. Intel. Lab. Syst. 2016. Vol. 151. Pр. 172–180.

Sena M.M., Trevisan M.G., Poppi R.J. Combining Standard Addition Method and Second-Order Advantage for Direct Determination of Salicylate in Undiluted Human Plasma by Spectrofluorimetry. Talanta. 2006. Vol. 68. Pр. 1707–1712.

Reguera C. Study of the Effect of the Presence of Silver Nanoparticles on Migration of Bisphenol A From Polycarbonate Glasses into Food Simulants. Chemom. Intel. Lab. Syst. 2018. Vol. 176. Pр. 66–73.

Spink J. The application of public policy theory to the emerging food fraud risk: next steps. Trends in Food Science & Technology. 2019. Vol. 85. Pр. 116–128.

Biletskyj E. V., Yanushkevych D. A., Shajkhlislamov Z. R. (2015) Upravlinnia iakistiu produktsii ta posluh: navchalnyj posibnyk. [Management of the quality of products and services: a study guide]. Kharkiv: KhTEI. (in Ukrainian)

Savuliak V. V. (2012) Upravlinnia iakistiu produktsii: navchalnyj posibnyk. [Product quality management: a study guide]. Vinnytsia: VNTU. (in Ukrainian)

Alewijn M., Vander Voet H., Van Ruth S. (2016) Validation of multivariate classification methods using analytical fingerprints-Concept and case study on organic feed for laying hens. Journal of Food Composition and Analysis, vol. 51, рр. 15–23.

Armstrong N., Hibbert D. B. (2009) An Introduction to Bayesian Methods for Analyzing Chemistry Data» Chemom. Intel. Lab. Syst, Part 1, vol. 97, рр. 194–210.

Medina S. (2019) Current trends and recent advances on food authenticity technologies and chemometric approaches. Trends in Food Science & Technology, vol. 85, рр. 163–176.

CX/FICS 18/24/7 (2018) «Discussion paper on food integrity and food authenticity». Codex committee on food import and export inspection and certification systems. Twenty-Fourth Session. Brisbane, Australia, October 22-26, 2018.

Delgado-Aguilar M., Valverde-Som L., Cuadros-Rodríguez L. (2018) Solver, an Excel Application to Solve the Difficulty in Applying Different Univariate Linear Regression Methods. Chemom. Intell. Lab. Syst, vol. 178, рр. 39–46.

Herrero A. (2002) Determination of the Capability of Detection of a Hyphenated Method: Application to Spectroelectrochemistry». Chemom. Intell. Lab. Syst, vol. 61 рр. 63–74.

Dong W., Zhang Y., Zhang B. (2012) Quantitative analysis of adulteration of extra virgin olive oil using Raman spectroscopy improved by bayesin framework least squares support vector machines. Analytical Methods, vol. 4, рр. 2772–2777.

Feinberg M. (2007) Validation of Analytical Methods Based on Accuracy Profiles. Journal of Chromatography A, vol. 1158, рр. 174–183.

García I., Sarabia L., Ortiz M. C., Aldama J. M. (2005) Usefulness of D-optimal Designs and Multicriteria Optimization in Laborious Analytical Procedures. Application to the Extraction of Quinolones From Eggs. Journal of Chromatography A, vol. 1085, рр. 190–198.

González A. G., Herrador M. A. (2006) Accuracy Profiles from Uncertainty Measurements. Talanta, vol. 70, рр. 896–901.

Knowledge Centre for Food Fraud and Quality. [Knowledge Center for Food Fraud and Quality]. Available at: https://knowledge4policy.ec.europa.eu/food-fraud-quality/topic/food-fraud_en.

Huch C.W., Pezzei C.K., Huck-Pezzei V.A.C. (2016) An industry pespective of food fraud. Current Opinion in Food Science, vol. 10, рр. 32–37.

Kumar N., Bansal A., Sarma G. S. (2014) Chemometrics tools in analytical chemistry: An overview. Talanta, vol. 123, рр. 186–199.

Maning L. (2016) Food Fraud: policy and food chain. Current Opinion in Food Science, vol. 10, рр. 16–21.

Ortiz M. C., Herrero A., Sanllorente S., Reguera C. (2005) The Quality of the Information Contained in Chemical Measures. [The Quality of the Information Contained in Chemical Measures]. Servicio de Publicaciones Universidad de Burgos. Burgos. Spain.

Ortiz M. C., Sarabia L. A., Sánchez M. S. (2010) Tutorial on Evaluation of Type I and type II Errors in Chemical Analyses: From the Analytical Detection to Authentication of Products and Process Control. Anal. Chim. Acta, vol. 674, рр. 123–142.

Ortiz M. C., Sarabia L. A., Sánchez M.S., Herrero A. (2020) Quality of Analytical Measurements: Statistical Methods for Internal Validation. Chemical and Biochemical Data Analysis, рр. 1–52.

Oca M. (2016) Robustness Testing in the Determination of Seven Drugs in Animal Muscle by Liquid Chromatography–Tandem Mass Spectrometry. Chemom. Intel. Lab. Syst, vol. 151, рр. 172–180.

Sena M. M., Trevisan M. G., Poppi R. J. (2006) Combining Standard Addition Method and Second-Order Advantage for Direct Determination of Salicylate in Undiluted Human Plasma by Spectrofluorimetry. Talanta, vol. 68, рр. 1707–1712.

Reguera C. (2018) Study of the Effect of the Presence of Silver Nanoparticles on Migration of Bisphenol A From Polycarbonate Glasses into Food Simulants. Chemom. Intel. Lab. Syst, vol. 176, рр. 66–73.

Spink J. (2019) The application of public policy theory to the emerging food fraud risk: next steps. Trends in Food Science & Technology, vol. 85, рр. 116–128.

Published
2023-09-26
How to Cite
Senyk, Y. (2023). STATISTICAL ANALYSIS OF THE RESULTS OF LABORATORY RESEARCH AS ONE OF THE METHODS OF INCREASING THE COMPETITIVENESS OF A MILK PROCESSING ENTERPRISE. Change Management and Innovation, (7), 50-57. https://doi.org/10.32782/CMI/2023-7-7